Gypsum was recovered using a direct flotation method, which included one roughing, one scavenging, and two cleaning operations, from −0.15 mm to +0.025 mm. The test results show that a gypsum concentrate with a CaSO 4 ·2H 2 O purity of 98.94%, CaSO 4 ·2H 2 O recovery of 80.02%, and whiteness of 37.05 was achieved.